HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 54477943, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 2-Amino-4,5,6,7,8-pentahydrothiazolo[5,4-d]azepine | HCID 19985785 | — |
| Reactant | 4-(3-Chloroprop-1-en-1-yl)-1,2-dimethoxybenzene | HCID 54481930 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 54477943 | HCID 54477943 | 7.7% |
Reaction Steps
Prepared from 3,4-dimethoxy-cinnamyl chloride (prepared at -5° C. for 10 minutes) and 2 equivalents of 2-amino-4,5,7,8-tetrahydro-6H-thiazolo[5,4-d]azepine in chloroform. Yield: 7.7% of theory, Melting point: 122°-126° C. (ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05068325 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-deeee94051c5410b8b38745d98536009 |
| Source note | uspto-grants-1991_11 |