HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-4,5,6,7,8-pentahydrothiazolo[5,4-d]azepine → HCID 73668870, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-4,5,6,7,8-pentahydrothiazolo[5,4-d]azepine | HCID 19985785 | — |
| Reactant | Chloroform methanol | HCID 21584188 | — |
| Reactant | HCID 54441900 | HCID 54441900 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 73668870 | HCID 73668870 | 31% |
Reaction Steps
Prepared from 3-(1-naphthyl)allyl chloride and 2 equivalents of 2-amino-4,5,7,8-tetrahydro-6 H-thiazolo[5,4-d]azepine in chloroform for 3 days at 20° C. Yield: 31% of theory, Melting point: 178°-180° C. (chloroform/methanol =100:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05068325 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-ef718ec902a045d194cd9221b549206e |
| Source note | uspto-grants-1991_11 |