HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 53732315, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 2-Amino-4,5,6,7,8-pentahydrothiazolo[5,4-d]azepine | HCID 19985785 | — |
| Reactant | HCID 53940112 | HCID 53940112 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 53732315 | HCID 53732315 | 36% |
Reaction Steps
Prepared from 2-benzyloxy-cinnamyl chloride and 2 equivalents of 2-amino-4,5,7,8-tetrahydro-6 H-thiazolo[5,4-d]azepine in chloroform for 5 hours at 50° C. Yield: 36% of theory, Melting point: 103°-107° C. (ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05068325 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-1aec29d0c35e453699581ae94d337cf4 |
| Source note | uspto-grants-1991_11 |