HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 54327587, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 2-Amino-4,5,6,7,8-pentahydrothiazolo[5,4-d]azepine | HCID 19985785 | — |
| Reactant | HCID 54206840 | HCID 54206840 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 54327587 | HCID 54327587 | 59% |
Reaction Steps
Prepared from 3-benzyloxy-cinnamyl chloride and 2 equivalents of 2-amino-4,5,7,8-tetrahydro-6 H-thiazolo[5,4-d]azepine in chloroform for 5 hours at 50° C. Yield: 59% of theory, Melting point: 78°-80° C. (ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05068325 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-7c1e6ee626be4be6861e104f5f41c37d |
| Source note | uspto-grants-1991_11 |