HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-4,5,6,7,8-pentahydrothiazolo[5,4-d]azepine → HCID 53886359, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-4,5,6,7,8-pentahydrothiazolo[5,4-d]azepine | HCID 19985785 | — |
| Reactant | (3-Chloro-2-methylprop-1-en-1-yl)benzene | HCID 54254060 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 53886359 | HCID 53886359 | 8% |
Reaction Steps
Prepared from 2-methyl-3-phenyl-allyl chloride and 2 equivalents of 2-amino-4,5,7,8-tetrahydro-6H-thiazolo[5,4-d]azepine in chloroform for 2 hours at ambient temperature. Yield: 8% of theory, Melting point: 112°-115° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05068325 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-c31b1d4aa55a4b36bb95216cb90f4fb8 |
| Source note | uspto-grants-1991_11 |