HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 54297882, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | 2-Amino-4,5,6,7,8-pentahydrothiazolo[5,4-d]azepine | HCID 19985785 | — |
| Reactant | HCID 70048082 | HCID 70048082 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 54297882 | HCID 54297882 | 22% |
Reaction Steps
Prepared from 3-(5-methyl-2-pyridyl)allyl chloride hydrochloride and 3 equivalents of 2-amino-4,5,7,8-tetrahydro-6H-thiazolo[5,4-d]azepine in chloroform. Yield: 22% of theory, Melting point: 172°-175° C. (isopropanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05068325 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-0853bf1f0b8e4fb396603f91da2a20c5 |
| Source note | uspto-grants-1991_11 |