HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 86745242, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | HCID 19985806 | HCID 19985806 | — |
| Catalyst | Pd barium sulfate | HCID 16218511 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86745242 | HCID 86745242 | 42% |
Reaction Steps
Prepared by catalytic hydrogenation of 2-amino-6 -(3-(3-pyridyl)-2-propyn-1-yl)-4,5,7,8-tetrahydro-6H-thiazolo[5,4-d]azepine with palladium/barium sulphate (5%) in ethanol. Yield: 42% of theory, Melting point: 125°-126° C. (acetone).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05068325 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-157bbe03b0b24f5f8ee5aaf7688deb47 |
| Source note | uspto-grants-1991_11 |