HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Pyridin-3-yl)acrylaldehyde → HCID 54319254, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Pyridin-3-yl)acrylaldehyde | HCID 309465 | — |
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Reactant | 2-Amino-4,5,6,7,8-pentahydrothiazolo[5,4-d]azepine | HCID 19985785 | — |
| Product | HCID 54319254 | HCID 54319254 | 40% |
Reaction Steps
Prepared from 3-(3-pyridyl)acrolein and 2-amino-4,5,7,8-tetrahydro-6H-thiazolo[5,4-d]azepine by reductive amination with sodium cyanoborohydride. Yield: 40% of theory, Melting point: 162°-165° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05068325 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-e03e85ecb75b4ed29b4662d9723dbb12 |
| Source note | uspto-grants-1991_11 |