HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 54375116, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 54327587 | HCID 54327587 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54375116 | HCID 54375116 | 71% |
Reaction Steps
Prepared from 2-amino-6-(3-(3-benzyloxy-phenyl)allyl)-4,5,7,8-tetrahydro-6H- thiazolo[5,4-d]azepine with 2 equivalents of boron tribromide in methylene chloride. Yield: 71% of theory, Melting point: 85°-95° C. (ether); foamy.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05068325 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-80801ff0fbdf4db5b5fa16fc0e2e8275 |
| Source note | uspto-grants-1991_11 |