HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropyl Ether → HCID 54240092, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Amino-4,5,6,7,8-pentahydrothiazolo[5,4-d]azepine | HCID 19985785 | — |
| Reactant | 1-Bromo-2-(3-bromo-1-propen-1-yl)benzene | HCID 53688271 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 54240092 | HCID 54240092 | 42% |
Reaction Steps
Prepared analogously to Example 1 from 2-amino-4,5,7,8-tetrahydro-6H-thiazolo[5,4-d]azepine, potassium carbonate and 2-bromo-cinnamyl bromide in anhydrous dimethylformamide for 2 hours at 20° C. Yield: 42% of theory, Melting point: 103°-106° C. (diisopropylether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05068325 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-ea78143dc56d4c898a458d47f0192369 |
| Source note | uspto-grants-1991_11 |