HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 54514614, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Amino-4,5,6,7,8-pentahydrothiazolo[5,4-d]azepine | HCID 19985785 | — |
| Reactant | HCID 54572020 | HCID 54572020 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 54514614 | HCID 54514614 | 41% |
Reaction Steps
Prepared analogously to Example 1 from 2-amino-4,5,7,8-tetrahydro-6H-thiazolo[5,4-d]azepine, potassium carbonate and 3-trifluoromethyl-cinnamyl bromide in anhydrous dimethylformamide for one hour at 20° C. Yield: 41% of theory, Melting point: 102°-105° C. (petroleum ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05068325 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-819ce6c86a8948829ab494635cf2eb1f |
| Source note | uspto-grants-1991_11 |