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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 974404Generated: October 29, 2026

Lithium diisopropylamide → HCID 178505776, compound

https://huagongshe.com/reaction/974404

Reaction equation

Participants

RoleNameHCIDCharge
ReactantLithium diisopropylamideHCID 2724682—
Reactant1-[(2,4-Difluorophenyl)methyl]-1H-pyrroleHCID 18972360—
ReactantHCID 178420582HCID 178420582—
ProductHCID 178505776HCID 17850577655.1%

Reaction Steps

Analogously to Example 19,2.5 g (0.010 mol)of bis(cyclopentadienyl)titanium dichloride and 4.25 g (0.022 mol) of 1-[(2,4-difluorophenyl)methyl]-1H-pyrrole are reacted with 0.022 mol of lithium diisopropylamide solution. 3.1 g of orange crystals melting point 192°-194° C. are obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05068371
Source datasetuspto-grants-1991_11
ORD IDord-291c0c3be6c6497bad6f6ee6a6bc1bdf
Source noteuspto-grants-1991_11