Sodium Bicarbonate → HCID 19969624, compound

Participants

Reaction Steps

The amine of step (b) (25 g) was dissolved in 1N HCl (300 ml) and stirred at room temperature overnight to hydrolyze the acetal group. The solution was neutralized with NaHCO3 and the amine was extracted into chloroform. Concentration of the chloroform afforded the subtitle compound (27 g) as a yellow solid.

Provenance & Evidence