Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → 1,2-Dimethyl-3-oxa-2,7-diazabicyclo[3.3.0]octane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 7-Acetyl-1,2-dimethyl-3-oxa-2,7-diazabicyclo[3.3.0]octane | HCID 15070017 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 1,2-Dimethyl-3-oxa-2,7-diazabicyclo[3.3.0]octane | HCID 15070018 | — |
반응 단계
11.8 g (64 mmol) of 7-acetyl-1,2-dimethyl-3-oxa-2,7-diazabicyclo[3.3.0]octane are heated under reflux with 12 g of NaOH in 36 ml of water overnight. The mixture is saturated with K2CO3 and extracted several times with CHCl3, the extract is dried over K2CO3 and concentrated and the residue is distilled.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05607942 |
| 출처 데이터셋 | uspto-grants-1997_03 |
| ORD ID | ord-f11e245f3cb44d96a943fda29de7d7c4 |
| 출처 메모 | uspto-grants-1997_03 |