HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19969794, compound → HCID 19969814, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19969794 | HCID 19969794 | — |
| Solvent | Methane | HCID 297 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Palladium | HCID 23938 | — |
| Product | HCID 19969814 | HCID 19969814 | — |
Reaction Steps
8.0 g (35 mmol) of 8-benzyl-4-methyl-2,8-diazabicyclo[4.3.0]nonane are dissolved in 60 ml of methanol and hydrogenated over palladium on active charcoal at 100° C. and under 100 bar. Then the catalyst is filtered off, the filtrate is concentrated by evaporation and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05607942 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-d823accfd9d042a894040d21ce51fcb5 |
| Source note | uspto-grants-1997_03 |