HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 19970307, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 2747423 | HCID 2747423 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 19970307 | HCID 19970307 | — |
Reaction Steps
17 g of N-(1-benzylpiperid-4-yl)-N'-tert-butylthiourea are added to 170 ml of 33% hydrobromic acid in acetic acid; the reaction mixture is stirred at room temperature for 4 hours, then it is poured over diethylether. The crystals obtained are filtered and they are thoroughly washed with diethylether in order to obtain white crystals which melt at 120° C.; yield: quantitative.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05607952 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-fb3d83763f6a4bdfacfaaf656bc33681 |
| Source note | uspto-grants-1997_03 |