3,4,5-Trichloroaniline → HCID 13749711, compound

HRID 975133Notes

Reaction equation

HRID 975133 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:6]=[C:7]([Cl:10])[C:8]=1[Cl:9])[NH2:5].[F:11][C:12]1[CH:22]=[CH:21][CH:20]=[C:19]([F:23])[C:13]=1[C:14]([N:16]=[C:17]=[O:18])=[O:15]>C1(C)C=CC=CC=1>[Cl:1][C:2]1[CH:3]=[C:4]([NH:5][C:17]([NH:16][C:14](=[O:15])[C:13]2[C:19]([F:23])=[CH:20][CH:21]=[CH:22][C:12]=2[F:11])=[O:18])[CH:6]=[C:7]([Cl:10])[C:8]=1[Cl:9]

Participants

4

Reactant 2

HCID 124693,4,5-TrichloroanilineHCID 27333692,6-Difluorobenzoyl isocyanate

Product 1

HCID 13749711HCID 13749711, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

3,4,5-trichloro-aniline (19.7 g) and 2,6-difluorobenzoyl isocyanate (18.3 g) were dissolved in toluene (200 ml) at 50° C., and the solution was allowed to stand at this temperature for five hours. After cooling the solution to room temperature, the title compound was isolated by suction filtration and dried.

Sources & evidence

ORD record
ord-2ab5ce52381d45488fd4addcab8b1d34
Source dataset
uspto-grants-1997_03
Patent number
US05607977

Reaction notes

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