HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4,5-Trichloroaniline → HCID 13749711, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4,5-Trichloroaniline | HCID 12469 | — |
| Reactant | 2,6-Difluorobenzoyl isocyanate | HCID 2733369 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 13749711 | HCID 13749711 | — |
Reaction Steps
3,4,5-trichloro-aniline (19.7 g) and 2,6-difluorobenzoyl isocyanate (18.3 g) were dissolved in toluene (200 ml) at 50° C., and the solution was allowed to stand at this temperature for five hours. After cooling the solution to room temperature, the title compound was isolated by suction filtration and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05607977 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-2ab5ce52381d45488fd4addcab8b1d34 |
| Source note | uspto-grants-1997_03 |