huagongshe.com
HRID975144

反应详情

EQUATION

反应方程式

HRID 975144 的结构方程式

REACTANTS

反应物

2
结构：C=CC(C)O
HCID11716

3-Buten-2-ol

C4H8O

结构：CN1CCC(c2c[nH]c3ccc(Br)cc23)CC1
HCID15745344

5-Bromo-3-(1-methylpiperidin-4-yl)-1H-indole

C14H17BrN2

PRODUCTS

生成物

1
结构：CC(O)C=Cc1ccc2[nH]cc(C3CCN(C)CC3)c2c1
HCID54086563

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Obtained by a procedure similar to that described in Example 1, using 5-bromo-3-(N-methyl-4-piperidyl)-1H-indole (EP-A-0303507) and but-3-en-2-ol, as a foam. Rf 0.50 (SS 4). Found: C,72.85; H,8.22; N,9.17. C18H24N2O; 0.17 CH2Cl2 requires C,73.08; H,8.22; N,9.38%.

WORKUP

后处理

  1. customObtained by a procedure similar to