HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(3-Hydroxy-1-but-1-enyl)-3-(N-methyl-4-piperidyl)-1H-indole → 5-(3-Hydroxy-1-butyl)-3-(N-methyl-4-piperidyl)-1H-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(3-Hydroxy-1-but-1-enyl)-3-(N-methyl-4-piperidyl)-1H-indole | HCID 54086563 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 5-(3-Hydroxy-1-butyl)-3-(N-methyl-4-piperidyl)-1H-indole | HCID 19970945 | — |
Reaction Steps
Obtained from the title compound of Example 42 by a procedure similar to that described in Example 2, but using 10% palladium on charcoal as catalyst, as a foam. Rf 0.50 (SS 4). C,73.39; H,8.77; N,9.06. C18H26N2O; 0.125 CH2Cl2 requires C,73.28; H,8.91; N,9.43%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05607960 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-631587a7f2de4c9a86ff6b175d215833 |
| Source note | uspto-grants-1997_03 |