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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 975147Generated: October 29, 2026

2-Methyl-3-buten-2-ol → 5-(3-Hydroxy-3-methyl-1-but-1-enyl)-3-(2-phthalimidoethyl)-1H-indole

https://huagongshe.com/reaction/975147

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Methyl-3-buten-2-olHCID 8257—
ReactantHCID 19970994HCID 19970994—
SolventDichloromethaneHCID 6344—
Product5-(3-Hydroxy-3-methyl-1-but-1-enyl)-3-(2-phthalimidoethyl)-1H-indoleHCID 53763526—

Reaction Steps

Obtained by a procedure similar to that described in Example 1, using 5-bromo-3-(2-phthalimidoethyl)-1H-indole (which was prepared as described in U.S. Pat. No. 4,252,803) and 2-methylbut-3-en-2-ol, as a foam. Rf 0.10 (SS 8). Found: C,72.31; H,6.09; N,.7.16. C23H22N2O3 ; 0.15 CH2Cl2 requires C,71.82; H,5.81; N,7.23%.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05607960
Source datasetuspto-grants-1997_03
ORD IDord-f6b5c56c0f29406aba0d3bda9fbf1fc2
Source noteuspto-grants-1997_03