HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-3-buten-2-ol → 5-(3-Hydroxy-3-methyl-1-but-1-enyl)-3-(2-phthalimidoethyl)-1H-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-3-buten-2-ol | HCID 8257 | — |
| Reactant | HCID 19970994 | HCID 19970994 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 5-(3-Hydroxy-3-methyl-1-but-1-enyl)-3-(2-phthalimidoethyl)-1H-indole | HCID 53763526 | — |
Reaction Steps
Obtained by a procedure similar to that described in Example 1, using 5-bromo-3-(2-phthalimidoethyl)-1H-indole (which was prepared as described in U.S. Pat. No. 4,252,803) and 2-methylbut-3-en-2-ol, as a foam. Rf 0.10 (SS 8). Found: C,72.31; H,6.09; N,.7.16. C23H22N2O3 ; 0.15 CH2Cl2 requires C,71.82; H,5.81; N,7.23%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05607960 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-f6b5c56c0f29406aba0d3bda9fbf1fc2 |
| Source note | uspto-grants-1997_03 |