HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 22870281, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 54069448 | HCID 54069448 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22870281 | HCID 22870281 | — |
Reaction Steps
Obtained from the title compound of Example 49 by a procedure similar to that described in Example 2, but using 10% palladium on charcoal as catalyst, as a foam. [α]D25 +83° (c=0.1, CH3OH). Found: C,71.61; H,8.36; N,9.02. C18H24N2O; 0.20 CH2Cl2 requires C,71.84; H,8.16; N,9.30%. LRMS: m/z 285.3 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05607960 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-2589e70868ec4c90845b8f746f67eb54 |
| Source note | uspto-grants-1997_03 |