HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 22870333, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 53988253 | HCID 53988253 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 22870333 | HCID 22870333 | — |
Reaction Steps
Obtained from the title compound of Example 96 by a procedure similar to that described in Example 2, but using 10% palladium on charcoal as catalyst, as a foam. Rf 0.40 (SS 7). Found: C,59.55; H,6.86; N,7.10. C19H25F3N2O; 0.17 CH2Cl2 ; H2O requires C,59.55; H,7.13; N,7.25%. LRMS: m/z 355.0 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05607960 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-12af266f0c0148669b5e64c58ac855d3 |
| Source note | uspto-grants-1997_03 |