Methanol → HCID 22870332, compound

Participants

Reaction Steps

Obtained from the title compound of Example 98 by a procedure similar to that described in Example 2, but using 10% palladium on charcoal as catalyst, as a foam. Rf 0.45 (SS 7). [α]D25 +39° (c=0.1, CH3OH). Found: C,59.07; H,7.16; N,9.21. C22H30F3N3O2 ; 0.05 CH2Cl2 ; H2O requires C,59.15; H,7.22; N,9.39%. LRMS: m/z 426.4 (M+1)+.

Provenance & Evidence