HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19972019, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 11071548 | HCID 11071548 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19972019 | HCID 19972019 | 97% |
Reaction Steps
An about 3N methanolic hydrochloric acid (10 ml) is added at room temperature with stirring to a solution of the bisalkylated phosphinic acid ester 10 (103 mg, 0.19 mol) in methanol (5 ml). After 3 hours, the reaction solution is concentrated under reduced pressure. The phosphinic acid ester hydrochloride 15 (69 mg, 97% of theory) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05608098 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-4e59333c25d64ca4a1ba6c10e068fcb2 |
| Source note | uspto-grants-1997_03 |