HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22376950, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Toluene | HCID 1140 | — |
| Reactant | HCID 11071548 | HCID 11071548 | — |
| Product | HCID 22376950 | HCID 22376950 | 93% |
Reaction Steps
A solution of the bisalkylated phosphinic acid ester 10 (170 mg, 0.32 mmol) in 37% aqueous hydrochloric acid (20 ml) is heated to a temperature of about 100° C. for 6 hours. After concentration of the reaction solution under reduced pressure and repeated coevaporation with methanol and toluene, the phosphinic acid hydrochloride 16 (101 mg, 93% of theory) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05608098 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-a11b849a8daa4d9a8334a1e97589d159 |
| Source note | uspto-grants-1997_03 |