HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19972094, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Reactant | HCID 53683221 | HCID 53683221 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19972094 | HCID 19972094 | — |
Reaction Steps
In 10 ml of methanol was suspended 0.30 g (0.59 mmole) of 2-[2-benzoylamino-l-(3-chlorophenyl)ethylidene]-N-(4-trifluoromethoxyphenyl)hydrazinecarboxamide, and 0.07 g (1 mmole) of sodium cyanoborohydride was added to the resulting suspension. The resulting mixture was adjusted to pH 4 to 6 with a methanolic solution of hydrogen chloride at room temperature and subjected to reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05608109 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-8db07af2006a49a38c38dd285c95bae6 |
| Source note | uspto-grants-1997_03 |