Hydrochloric Acid → HCID 19972088, compound

Participants

Reaction Steps

In 10 ml of methanol was suspended 0.50 g (1.2 mmoles) of 2-[2-(2-propynylthio)-1-phenylethylidene]-N-(4-trifluoromethoxyphenyl)hydrazinecarboxamide, and 0.37 g (4.7 mmoles) of sodium cyanoborohydride was added to the resulting suspension. The resulting mixture was adjusted to pH 4 to 6 with a methanolic solution of hydrogen chloride at room temperature and subjected to reaction.

Provenance & Evidence