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HRID975796

反应详情

EQUATION

反应方程式

HRID 975796 的结构方程式

REACTANTS

反应物

2
结构：O=C1Nc2cccnc2N(C(=O)CCl)c2ccccc21
HCID120053

11-(Chloroacetyl)-5,11-dihydro-6H-pyrido(2,3-b)(1,4)benzodiazepin-6-one

C14H10ClN3O2

结构：O=C(CNCCCC1CCCNC1)c1ccccc1
HCID19039430

未命名化合物

PRODUCTS

生成物

1
结构：O=C(CNCCCC1CCCN(CC(=O)N2c3ccccc3C(=O)Nc3cccnc32)C1)c1ccccc1
HCID19039392

未命名化合物

PROCEDURE

实验过程

Prepared analogously to Example 8 from 11-(chloroacetyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]-benzodiazepin-6-one and 3-[3-[(benzoyl)methylamino]-propyl]piperidine. Purification is carried out by chromatography on silica gel using a mixture of methylene chloride/methanol=99:1 as eluant.

WORKUP

后处理

  1. customPurification
  2. additiona mixture of methylene chloride/methanol=99:1 as eluant