HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron, trihydro(thiobis(methane))-, (T-4)- → 9,10-dihydro-4H-pyrrolo[1,2-a]thieno[2,3-e][1,4]diazepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron, trihydro(thiobis(methane))-, (T-4)- | HCID 9833925 | — |
| Reactant | 9-oxo-9,10-dihydro-4H-pyrrolo[1,2-a]-thieno[2,3-e][1,4]diazepine | HCID 11041864 | — |
| Product | 9,10-dihydro-4H-pyrrolo[1,2-a]thieno[2,3-e][1,4]diazepine | HCID 21837159 | — |
Reaction Steps
The synthesis of 9-oxo-9,10-dihydro-4H-pyrrolo[1,2-a]thieno[2,3-e][1,4]diazepine is reported by A. Daich and B. Decroix, Bull. Soc. Chim. Fr 129, 360(1992); ##STR104## and is reduced with boron-dimethylsulfide to give 9,10-dihydro-4H-pyrrolo [1,2-a]thieno [2,3-e][1,4]diazepine. ##STR105##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05610156 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-deb72b1486a1402fba731c855093e59f |
| Source note | uspto-grants-1997_03 |