Hydrochloric Acid → HCID 86750549, compound

HRID 976012Notes

Reaction equation

HRID 976012 reaction equation
C[O:2][C:3](=[O:16])[C@@H:4]([NH2:15])[CH2:5]/[CH:6]=[CH:7]/[CH2:8][C@H:9]([NH2:14])[C:10]([O:12]C)=[O:11].[ClH:17]>>[ClH:17].[ClH:17].[NH2:15][C@@H:4]([CH2:5]/[CH:6]=[CH:7]/[CH2:8][C@H:9]([NH2:14])[C:10]([OH:12])=[O:11])[C:3]([OH:16])=[O:2]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 71474603(S,S)-2,7-Diamino-(E)-oct-4-ene-1,8-dioic acid dimethyl ester

Product 1

HCID 86750549HCID 86750549, compound

Procedure

(S,S)-2,7-Diamino-(E)-oct-4-ene-1,8-dioic acid dimethyl ester (1.65 g, 7.17 mmol) was heated under reflux with 6H HCl (10 ml, 60 mmol) for 2 hours. The solvent was then evaporated, the residue was dissolved in water (10 ml) and ethanol was added (100 ml). The white crystals were filtered off and dried in vacuum at 40° C.

Workup

  1. customThe solvent was then evaporated
  2. dissolutionthe residue was dissolved in water (10 ml)
  3. additionethanol was added (100 ml)
  4. filtrationThe white crystals were filtered off
  5. customdried in vacuum at 40° C.

Sources & evidence

ORD record
ord-e3de0dc4f3034c94952d772f35754d99
Source dataset
uspto-grants-1997_03
Patent number
US05610141

Reaction notes

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