HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 15177067, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 15177066 | HCID 15177066 | — |
| Product | HCID 15177067 | HCID 15177067 | 100% |
Reaction Steps
A solution of 1.5 9 (5.2 mmol) of 2-(1-naphthylmethyl)-2-benzylacetic acid in 10 mL SOCl2 was stirred at room temperature overnight. The SOCl2 was removed under reduced pressure, the residue taken up in Et2O, and the solvent again removed under reduced pressure to give 1.6 g (100% yield) of the product as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05610177 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-0a518134b5ac498c998a3e5976ff3813 |
| Source note | uspto-grants-1997_03 |