Acetic Anhydride → HCID 54498287, compound

Participants

Reaction Conditions

Reaction Steps

To 0.17 g of N-(5,6-dihydro-7H-cyclopenta[d]pyrimidin-4-yl)-4-(3-[1-(2-aminobenzyl)piperidin-4-yl]propanoyl)aniline were added 30 ml of chloroform, 1 ml of acetic anhydride and 0.38 g of 4-dimethylaminopyridine, and the mixture was stirred at 50° C. for 10 minutes. Then, the solvent was removed by distillation under reduced pressure and the obtained residue was applied to silica gel column chromatography to obtain 0.06 g of the title compound as white crystal.

Provenance & Evidence