HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178501833, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178451370 | HCID 178451370 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178501833 | HCID 178501833 | — |
Reaction Steps
Hydrochloric acid gas is piped for an hour over a solution of 59.4 g of tert.butyl (trans-4-aminocyclohexyl)oxyacetate in 500 ml of methanol, cooled in an ice bath, and then the mixture is stirred overnight at ambient temperature. It is evaporated to dryness, the residue is triturated with acetone and the solid is suction filtered and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05612335 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-78f9cc1f0fb44aff9dfe05c9f3b79710 |
| Source note | uspto-grants-1997_03 |