HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 19955567, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Chloroacetic anhydride | HCID 10946 | — |
| Reactant | HCID 19967241 | HCID 19967241 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 19955567 | HCID 19955567 | — |
Reaction Steps
The title compound of example F is treated with trifluoroacetic acid in methylene chloride at room temperature. The volatiles are removed under reduced pressure to afford a residue which is treated with chloroacetic anhydride and triethylamine. The chloroacetylated material is then reacted with NaI in acetone to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05612366 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-ea9cb383a9694305a781a2c308e30aed |
| Source note | uspto-grants-1997_03 |