HuagongsheHuagongshe Chemistry Print Report · For research reference only
98061-65-5 → HCID 86750586, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 98061-65-5 | HCID 6023270 | — |
| Reactant | HCID 178526132 | HCID 178526132 | — |
| Product | HCID 86750586 | HCID 86750586 | 67% |
Reaction Steps
The (Z)-2-bromomethyl-3-phenylpropenoic acid described in Example 1 (step A) is reacted with thiobenzoic acid according to the experimental procedure described in Example 1 (step B). Yield=67% (recrystallized in ether) m.p. 160° C. 1H NMR CDCl3 /TMS): 8.15 to 7.80 (m, 3H); 7.70 to 7.20 (m, 8H); 4.20 (s, 2H)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05612371 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-0ceeb50cb90e469a8848071a270744aa |
| Source note | uspto-grants-1997_03 |