4-Bromophenyl isocyanate → HCID 19967431, compound

Participants

Reaction Steps

Using the method of Compound 39 Part C, N-(1-ethylpropyl)hydroxylamine (2.6 g, 25 mmol) was reacted with 4-bromophenyl isocyanate (5 g, 25 mmol) to provide 2.1 g of the desired product as a solid, m.p. 129°-131° C. Analysis: Calculated for C12H17BrN2O2 : %C, 47.86; %H, 5.69; %N, 9.3; Found: %C, 47.79; %H, 5.54; %N, 9.25.

Provenance & Evidence