4-Bromophenyl isocyanate → HCID 19967431, compound

HRID 976622Notes

Reaction equation

HRID 976622 reaction equation
[CH2:1]([CH:3]([NH:6][OH:7])[CH2:4][CH3:5])[CH3:2].[Br:8][C:9]1[CH:14]=[CH:13][C:12]([N:15]=[C:16]=[O:17])=[CH:11][CH:10]=1>>[Br:8][C:9]1[CH:14]=[CH:13][C:12]([NH:15][C:16](=[O:17])[N:6]([CH:3]([CH2:4][CH3:5])[CH2:1][CH3:2])[OH:7])=[CH:11][CH:10]=1

Participants

3

Reactant 2

HCID 756094-Bromophenyl isocyanateHCID 19073513N-(pentan-3-yl)hydroxylamine2×

Product 1

HCID 19967431HCID 19967431, compound

Procedure

Using the method of Compound 39 Part C, N-(1-ethylpropyl)hydroxylamine (2.6 g, 25 mmol) was reacted with 4-bromophenyl isocyanate (5 g, 25 mmol) to provide 2.1 g of the desired product as a solid, m.p. 129°-131° C. Analysis: Calculated for C12H17BrN2O2 : %C, 47.86; %H, 5.69; %N, 9.3; Found: %C, 47.79; %H, 5.54; %N, 9.25.

Sources & evidence

ORD record
ord-79a1a2f63d714467be7d6e4645b7e548
Source dataset
uspto-grants-1997_03
Patent number
US05612377

Reaction notes

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