HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 19967571, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 6-Methoxy-2-(methylsulfanyl)pyrimidin-4-amine | HCID 4121981 | — |
| Product | HCID 19967571 | HCID 19967571 | 60% |
Reaction Steps
The compound soluble in ether was 2-methylmercapto-4-amino-6-methoxypyrimidine. This compound was removed from the solid residue by repeated washings with ether and filtering out of the solid residue. The solid residue was then recrystallized from alcohol to give 43 as slender prisms (yield=60%, m.p. 255° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05612468 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-cec0871f8b22467e8d18aa638134161a |
| Source note | uspto-grants-1997_03 |