HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → HCID 14745383, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Trichloroacetyl isocyanate | HCID 76400 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 14745383 | HCID 14745383 | — |
Reaction Steps
4.7 g (0.05 mol) of phenol are dissolved in a mixture of 10 g of water and 10 g of acetone. 9.4 g (0.05 mol) of trichloroacetyl isocyanate are subsequently added dropwise over the course of 30 minutes. The mixture is stirred at room temperature for 30 minutes and under reflux for 2.5 hours. The solvent mixture is evaporated in a rotary evaporator, and the solid obtained is recrystallized from DMSO.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05614351 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-9983c0be205c45a1bdab269d782235cc |
| Source note | uspto-grants-1997_03 |