HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 86750593, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 19964379 | HCID 19964379 | — |
| Product | HCID 86750593 | HCID 86750593 | — |
Reaction Steps
A suspension of 14 g (43.3 mmol ) of 10-methoxy-8-oxo-5,8,13,13a-tetrahydro-6H-dibenzo[a,g]quinolizine-13-carboxylic acid in 100 ml of methanol is prepared in a 500 ml three-necked round-bottomed flask, 3.2 ml (44.11 mmol) of thionyl chloride are added dropwise and the mixture is heated to reflux for 4 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05614517 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-087a6d32b33d472d96d40c1361e87486 |
| Source note | uspto-grants-1997_03 |