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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 977074Generated: October 29, 2026

HCID 86750595, compound → HCID 86750594, compound

https://huagongshe.com/reaction/977074

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86750595HCID 86750595—
SolventTolueneHCID 1140—
ProductHCID 86750594HCID 86750594—

Reaction Steps

5.5 g (15.13 mmol) of methyl (E)-3-(10-methoxy-8-oxo-5,8,13,13a-tetrahydro-6H-dibenzo[a,g]quinolizin-13-yl)prop-2-enoate are dissolved in 150 ml of toluene in a 500 ml round-bottomed flask, 5.15 g (22.7 mmol) of 2,3-dichloro-5,6-dicyanocyclohexa-2,5-diene-1,4-diene are added and the mixture is heated at reflux for 2 h 30.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05614517
Source datasetuspto-grants-1997_03
ORD IDord-d9b91f49868343afaa01ef64ed382df0
Source noteuspto-grants-1997_03