HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86750595, compound → HCID 86750594, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86750595 | HCID 86750595 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86750594 | HCID 86750594 | — |
Reaction Steps
5.5 g (15.13 mmol) of methyl (E)-3-(10-methoxy-8-oxo-5,8,13,13a-tetrahydro-6H-dibenzo[a,g]quinolizin-13-yl)prop-2-enoate are dissolved in 150 ml of toluene in a 500 ml round-bottomed flask, 5.15 g (22.7 mmol) of 2,3-dichloro-5,6-dicyanocyclohexa-2,5-diene-1,4-diene are added and the mixture is heated at reflux for 2 h 30.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05614517 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-d9b91f49868343afaa01ef64ed382df0 |
| Source note | uspto-grants-1997_03 |