HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2-bromoacetyl)benzoic Acid → HCID 67712514, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2-bromoacetyl)benzoic Acid | HCID 2756836 | — |
| Reactant | 2-Aminoisonicotinonitrile | HCID 7015524 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67712514 | HCID 67712514 | — |
Reaction Steps
8.5 g of 2-amino-4-cyanopyridine and 27.5 g of 4-bromoacetylbenzoic acid are boiled in 260 ml of ethanol for 20 h. After cooling, the precipitate is filtered off with suction and subjected to the customary working-up. 4-(7-Cyanoimidazo[1,2-a]pyridin-2-yl)benzoic acid hydrobromide is obtained, m.p. >310°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05614531 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-2d441bdfff8c4b6f80a64eb6948a9912 |
| Source note | uspto-grants-1997_03 |