HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetate → HCID 131719940, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetate | HCID 175 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 3-{1-[3-(4-Tert-butoxycarbonylaminomethylphenyl)-2-oxo-5-oxazolidinylcarbonyl]-4-piperazinyl}propionic acid | HCID 19965488 | — |
| Product | HCID 131719940 | HCID 131719940 | — |
Reaction Steps
0.43 g of 3-{1-[3-(4-tert-butoxycarbonylaminomethylphenyl)-2-oxo-5-oxazolidinylcarbonyl]-4-piperazinyl}propionic acid, acetate, is stirred in 30 ml of ethereal HCl solution at room temperature. The precipitate formed is filtered off with suction, washed with a little ether and dried. 3-{1-[3-(4-aminomethylphenyl)-2-oxo-5-oxazolidinylcarbonyl]-4-piperazinyl}propionic acid, dihydrochloride, is obtained, m.p. 184°-186°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05614535 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-d90db408527948a6b84d131e63b4a8f9 |
| Source note | uspto-grants-1997_03 |