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HRID977220

反应详情

EQUATION

反应方程式

HRID 977220 的结构方程式

REACTANTS

反应物

3
结构：CC(=O)[O-]
HCID175

Acetate

C2H3O2-

结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CC(C)(C)OC(=O)NCc1ccc(N2CC(C(=O)N3CCN(CCC(=O)O)CC3)OC2=O)cc1
HCID19965488

未命名化合物

PRODUCTS

生成物

1
结构：Cl.Cl.NCc1ccc(N2CC(C(=O)N3CCN(CCC(=O)O)CC3)OC2=O)cc1
HCID131719940

未命名化合物

PROCEDURE

实验过程

0.43 g of 3-{1-[3-(4-tert-butoxycarbonylaminomethylphenyl)-2-oxo-5-oxazolidinylcarbonyl]-4-piperazinyl}propionic acid, acetate, is stirred in 30 ml of ethereal HCl solution at room temperature. The precipitate formed is filtered off with suction, washed with a little ether and dried. 3-{1-[3-(4-aminomethylphenyl)-2-oxo-5-oxazolidinylcarbonyl]-4-piperazinyl}propionic acid, dihydrochloride, is obtained, m.p. 184°-186°.

WORKUP

后处理

  1. customThe precipitate formed
  2. filtrationis filtered off with suction
  3. washwashed with a little ether
  4. customdried