Triphenylphosphine → HCID 21840259, compound

HRID 977246Notes

Reaction equation

HRID 977246 reaction equation
[Cl:1][CH2:2][C:3]1[N:4]=[C:5]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[O:6][C:7]=1[CH3:8].[C:15]1([P:21]([C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)[C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[Cl-:1].[CH3:8][C:7]1[O:6][C:5]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[N:4][C:3]=1[CH2:2][P+:21]([C:22]1[CH:23]=[CH:24][CH:25]=[CH:26][CH:27]=1)([C:28]1[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=1)[C:15]1[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=1

Participants

3

Reactant 2

HCID 11776TriphenylphosphineHCID 97942894-(Chloromethyl)-5-methyl-2-phenyl-1,3-oxazole

Product 1

HCID 21840259HCID 21840259, compound

Procedure

4-Chloromethyl-5-methyl-2-phenyloxazole and triphenylphosphine were reacted in the same manner as in Reference Example 7 to yield (5-methyl-2-phenyl-4-oxazolylmethyl)triphenylphosphonium chloride. Melting point 277°-278° C.

Sources & evidence

ORD record
ord-cc3924b2926f4f288bbceaf28b62e832
Source dataset
uspto-grants-1997_03
Patent number
US05614544

Reaction notes

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