Triphenylphosphine → HCID 19965660, compound

HRID 977247Notes

Reaction equation

HRID 977247 reaction equation
[Cl:1][CH2:2][C:3]1[S:4][C:5]([CH3:14])=[C:6]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[N:7]=1.[C:15]1([P:21]([C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)[C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[Cl-:1].[CH3:14][C:5]1[S:4][C:3]([CH2:2][P+:21]([C:22]2[CH:23]=[CH:24][CH:25]=[CH:26][CH:27]=2)([C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)[C:15]2[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=2)=[N:7][C:6]=1[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1

Participants

3

Reactant 2

HCID 11776TriphenylphosphineHCID 199656082-(Chloromethyl)-5-methyl-4-phenylthiazole

Product 1

HCID 19965660HCID 19965660, compound

Procedure

2-Chloromethyl-5-methyl-4-phenylthiazole and triphenylphosphine were reacted in the same manner as in Reference Example 7 to yield (5- methyl-4-phenyl-2-thiazolylmethyl)triphenylphosphonium chloride. Melting point 256°-257° C.

Sources & evidence

ORD record
ord-e046b77b1b6c4526b73380a126bcf839
Source dataset
uspto-grants-1997_03
Patent number
US05614544

Reaction notes

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