HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Bicarbonate → HCID 131719944, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 131719151 | HCID 131719151 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 131719944 | HCID 131719944 | — |
Reaction Steps
2.53 g (4.6 mmol) of diastereomer mixture from Example 1 were taken up in a mixture of ethyl acetate and 5% strength aq. NaHCO3 solution and stirred for 5 min. The phases were separated, and the organic phase was washed with satd. aq. NaCl solution, dried with MgSO4 and concentrated in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05614623 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-44469b49fe5f49cc929f3b4bafaaa39f |
| Source note | uspto-grants-1997_03 |