反应详情

2.53 g (4.6 mmol) of diastereomer mixture from Example 1 were taken up in a mixture of ethyl acetate and 5% strength aq. NaHCO3 solution and stirred for 5 min. The phases were separated, and the organic phase was washed with satd. aq. NaCl solution, dried with MgSO4 and concentrated in vacuo.

1. customThe phases were separated
2. washthe organic phase was washed with satd
3. dry with materialaq. NaCl solution, dried with MgSO4
4. concentrationconcentrated in vacuo