Ethylene Glycol → HCID 19966073, compound

Participants

Reaction Steps

Following a procedure similar to that described in Preparation 1(ii), but using N-(2-isopropyl-6-chloromethylphenyl)-2-(9H-xanthen-9-yl)acetamide [prepared as described in Preparation 28(iv)] and ethylene glycol as starting materials, in relative amounts similar to those used in that Preparation, the title compound, melting at 153°-154° C. (after recrystallization from a mixture of diethyl ether and hexane), was obtained in a 52% yield.

Provenance & Evidence